5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride

Base Information

• Chemical Name: 5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride
• CAS No.: 83402-82-8
• Molecular Formula: C₁₁H₁₅NO₂*ClH
• Molecular Weight: 229.707
• Hs Code.: 2922199090
• European Community (EC) Number: 676-014-1
• DSSTox Substance ID: DTXSID70700666
• Mol file: 83402-82-8.mol

Synonyms:83402-82-8;5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride;5,6-Dimethoxy-1-aminoindane HCl;5,6-DIMETHOXY-INDAN-1-YLAMINE HYDROCHLORIDE;MFCD09878806;5,6-Dimethoxy-indan-1-ylamine, HCl;5,6-dimethoxy-2,3-dihydro-1H-inden-1-amine;hydrochloride;SCHEMBL17910635;DTXSID70700666;YULANTAURATVCM-UHFFFAOYSA-N;AKOS027327670;SB80402;AS-37623;5,6-dimethoxy-1-aminoindane hydrochloride;CS-0172546;EN300-7383861;A915594;Z3244816235;5,6-Dimethoxy-2,3-dihydro-1H-inden-1-aminehydrochloride;5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine--hydrogen chloride (1/1)

Chemical Property of 5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride

Chemical Property:

• Vapor Pressure: 0.001mmHg at 25°C
• Melting Point: 249-250 °C
• Refractive Index: 1.548
• Boiling Point: 301.135°C at 760 mmHg
• Flash Point: 148.141°C
• PSA: 44.48000
• Density: 1.11g/cm³
• LogP: 3.15210
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 229.0869564
• Heavy Atom Count: 15
• Complexity: 198

Purity/Quality:

97% ^*data from raw suppliers

5,6-Dimethoxy-1-aminoindaneHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=C(C=C2C(CCC2=C1)N)OC.Cl

Technology Process of 5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride

There total 3 articles about 5,6-Dimethoxy-2,3-dihydro-1H-inden-1-amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-azido-5,6-dimethoxy-2,3-dihydro-1H-indene (1560653-06-6) → 1-amino-5,6-dimethoxyindane hydrochloride (83402-82-8)

Guidance literature:

With palladium on activated charcoal; hydrogen; In methanol; chloroform; at 25 ℃; for 20h;

DOI:10.3109/14756366.2012.750311

Reference yield:

5,6-dimethoxy-1-indanone (2107-69-9) → 1-amino-5,6-dimethoxyindane hydrochloride (83402-82-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 3 h / 0 - 25 °C

2: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 14 h / 0 - 25 °C / Inert atmosphere

3: palladium on activated charcoal; hydrogen / methanol; chloroform / 20 h / 25 °C

With sodium tetrahydroborate; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; chloroform;

DOI:10.3109/14756366.2012.750311

Reference yield:

5,6-dimethoxy-2,3-dihydro-1H-inden-1-ol (33884-52-5) → 1-amino-5,6-dimethoxyindane hydrochloride (83402-82-8)

Guidance literature:

Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 14 h / 0 - 25 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen / methanol; chloroform / 20 h / 25 °C

With diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; chloroform;

DOI:10.3109/14756366.2012.750311

upstream raw materials:

1-azido-5,6-dimethoxy-2,3-dihydro-1H-indene

5,6-dimethoxy-1-indanone

5,6-dimethoxy-2,3-dihydro-1H-inden-1-ol

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