3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

Base Information

Chemical Name:3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide
CAS No.:1361189-60-7
Molecular Formula:C₁₅H₁₆BrN₃O₂
Molecular Weight:350.215
Hs Code.:

Synonyms:3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

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Chemical Property of 3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

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Technology Process of 3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

There total 3 articles about 3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5781-53-3
monomethyl oxalyl chloride

: 100481-08-1
oxo-pyrrolidin-1-yl-acetyl chloride

: 1361189-45-8
1-(4-bromophenyl)-N-hydroxycyclobutanecarboxamidine

: 1361189-60-7
3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

Guidance literature:: monomethyl oxalyl chloride; oxo-pyrrolidin-1-yl-acetyl chloride; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 ℃; for 0.5h;

1-(4-bromophenyl)-N-hydroxycyclobutanecarboxamidine; With pyridine; In tetrahydrofuran; at 50 ℃;

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 1361189-60-7
3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

1.2: 2 h / 0 °C

2.1: hydroxylamine / ethanol; water / 80 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 0 °C

3.2: 50 °C

With hydroxylamine; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 485828-58-8
1-(4- bromophenyl)cyclobutane-1-carbonitrile

: 1361189-60-7
3-[1-(4-bromo-phenyl)-cyclobutyl]-cyclopenta-1,3-dienecarboxylic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine / ethanol; water / 80 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0.5 h / 0 °C

2.2: 50 °C

With hydroxylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; water;