Technology Process of C26H29Cl2N3O6
There total 13 articles about C26H29Cl2N3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 7 steps
1.1: sodium dihydrogenphosphate; sodium chlorite; dihydrogen peroxide / acetonitrile; water / 24.5 h / 15 - 20 °C
2.1: thionyl chloride / 6 h / Reflux
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C
3.2: 1.5 h / 10 - 20 °C
4.1: hydrazine hydrate / ethanol / 2 h / Reflux
5.1: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
6.1: ammonium fluoride / water; ethanol / 48 h / 45 °C
7.1: hydrogenchloride / water; ethanol / 12 h / 20 °C
With
hydrogenchloride; ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate; thionyl chloride; dihydrogen peroxide; sodium hydride; hydrazine hydrate; triethylamine;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.bmcl.2012.11.058
- Guidance literature:
-
Multi-step reaction with 8 steps
1: aluminum (III) chloride / dichloromethane / 15 h / Reflux
2: sodium tetrahydroborate; acetic acid / 1 h / 10 °C
3: dichloromethane / 10 h / 20 °C
4: sodium tetrahydroborate / methanol / 1 h / 0 - 20 °C
5: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C
6: triethylamine / N,N-dimethyl-formamide / 24 h / 65 °C
7: ammonium fluoride / water; ethanol / 48 h / 45 °C
8: hydrogenchloride / water; ethanol / 12 h / 20 °C
With
1H-imidazole; hydrogenchloride; aluminum (III) chloride; ammonium fluoride; sodium tetrahydroborate; acetic acid; triethylamine;
In
methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.11.058