C₂₃H₂₅ClN₆O₄S

Base Information

Chemical Name:C₂₃H₂₅ClN₆O₄S
CAS No.:1353625-23-6
Molecular Formula:C₂₃H₂₅ClN₆O₄S
Molecular Weight:517.008
Hs Code.:

C<sub>23</sub>H<sub>25</sub>ClN<sub>6</sub>O<sub>4</sub>S

Synonyms:C₂₃H₂₅ClN₆O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₅ClN₆O₄S

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Technology Process of C₂₃H₂₅ClN₆O₄S

There total 9 articles about C₂₃H₂₅ClN₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: (x)C₂HF₃O₂*C₂₃H₂₇ClN₆O₄S

: 1353625-23-6
C₂₃H₂₅ClN₆O₄S

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 3h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353625-23-6
C₂₃H₂₅ClN₆O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: caesium carbonate / 17 h / 130 °C

5.1: trichlorophosphate / 2 h / 100 °C

6.1: HATU / N,N-dimethyl-formamide / 1 h

7.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 70 °C

8.1: Dess-Martin periodane / dichloromethane / 3 h

With sodium bis(trimethylsilyl)amide; hydrazinium monoacetate; caesium carbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In tetrahydrofuran; hexanes; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353625-23-6
C₂₃H₂₅ClN₆O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: caesium carbonate / 17 h / 130 °C

4.1: trichlorophosphate / 2 h / 100 °C

5.1: HATU / N,N-dimethyl-formamide / 1 h

6.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.5 h / 70 °C

7.1: Dess-Martin periodane / dichloromethane / 3 h

With sodium bis(trimethylsilyl)amide; hydrazinium monoacetate; caesium carbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;