2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

Base Information

Chemical Name:2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline
CAS No.:182559-77-9
Molecular Formula:C₁₉H₂₁NO₄
Molecular Weight:327.38
Hs Code.:

Synonyms:2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

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Technology Process of 2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

There total 3 articles about 2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 182559-77-9
2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

Guidance literature:

Reference yield:

: 198417-15-1
ethyl 1-benzyl-2,4-dioxopiperidine-3-carboxylate

: 182559-77-9
2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 9.64 g / potassium tert-butoxide / benzene; 2-methyl-propan-2-ol / 7 h / 70 - 80 °C

2: 1.) pyrrolidine, 2.) acetic acid, sodium acetate / 1.) benzene, reflux, 4 h, 2.) water, 100 deg C, 3 h

With pyrrolidine; potassium tert-butylate; sodium acetate; acetic acid; In tert-butyl alcohol; benzene;
DOI:10.3987/com-97-8023

Reference yield:

: 198417-18-4
1-Benzyl-2,4-dioxo-3-(3-oxo-butyl)-piperidine-3-carboxylic acid ethyl ester

: 182559-77-9
2-benzyl-8a-carboethoxy-1,6-dioxo-1,2,3,4,6,7,8,8a-octahydroisoquinoline

Guidance literature:: With pyrrolidine; sodium acetate; acetic acid; Yield given. Multistep reaction; 1.) benzene, reflux, 4 h, 2.) water, 100 deg C, 3 h;
DOI:10.3987/com-97-8023