Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

Base Information

Chemical Name:Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate
CAS No.:108290-93-3
Molecular Formula:C₂₃H₃₂N₂O₅
Molecular Weight:416.517
Hs Code.:

Synonyms:Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

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Technology Process of Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

There total 4 articles about Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50551-10-5
ethyl amidinoacetate

: 108290-93-3
Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / ethyl acetate / 0.33 h / Heating

2: 1.) NaH / 1.) DMF, O deg C - room temp. 1 h 2.) 0 deg C, 10 min

3: 1.) NaH / 1.) DMF, O deg C - room temp. 3 h 2.) 0 deg C, 2 h

4: 1.) NaH / 1.) DMF, 35 - 40 deg C, 3 h 2.) -20 deg C - room temp.

With sodium hydride; In ethyl acetate;
DOI:10.1002/jhet.5570230560

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 108290-93-3
Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, O deg C - room temp. 1 h 2.) 0 deg C, 10 min

2: 1.) NaH / 1.) DMF, O deg C - room temp. 3 h 2.) 0 deg C, 2 h

3: 1.) NaH / 1.) DMF, 35 - 40 deg C, 3 h 2.) -20 deg C - room temp.

With sodium hydride;
DOI:10.1002/jhet.5570230560

Reference yield:

: 108290-85-3
ethyl 2-amino-5-methyl-1H-pyrrole-3-carboxylate

: 108290-93-3
Ethyl N<1-Benzyloxymethyl-3-carbethoxy-5-methyl-2-pyrryl>-N'-ethyl-3-aminopropionate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, O deg C - room temp. 1 h 2.) 0 deg C, 10 min

2: 1.) NaH / 1.) DMF, O deg C - room temp. 3 h 2.) 0 deg C, 2 h

3: 1.) NaH / 1.) DMF, 35 - 40 deg C, 3 h 2.) -20 deg C - room temp.

With sodium hydride;
DOI:10.1002/jhet.5570230560