N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

Base Information

Chemical Name:N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide
CAS No.:1448857-94-0
Molecular Formula:C₂₂H₂₉N₃O₂
Molecular Weight:367.491
Hs Code.:

Synonyms:N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

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Technology Process of N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

There total 5 articles about N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 36394-07-7
5-hexenoyl chloride

: 1448858-09-0
5-(2-(hex-5-enyloxy)phenyl)-1-methyl-1H-imidazol-2-amine

: 1448857-94-0
N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

Guidance literature:: With pyridine; In dichloromethane; at -10 - 20 ℃;
DOI:10.1021/jm400287v

Reference yield:

: 1448858-12-5
1-(2-(hex-5-enyloxy)phenyl)ethanone

: 1448857-94-0
N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: DBBA; hydrogenchloride / diethyl ether; 1,4-dioxane / 1 h / 20 °C

2.1: acetonitrile / 0.58 h / 150 °C / Microwave irradiation

2.2: 0.17 h / 100 °C / Microwave irradiation

3.1: pyridine / dichloromethane / -10 - 20 °C

With pyridine; hydrogenchloride; DBBA; In 1,4-dioxane; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jm400287v

Reference yield:

: 64818-36-6
5-hexenyl methanesulfonate

: 1448857-94-0
N-(5-(2-(hex-5-en-1-yloxy)phenyl)-1-methyl-1H-imidazol-2-yl)hex-5-enamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 - 70 °C

2.1: DBBA; hydrogenchloride / diethyl ether; 1,4-dioxane / 1 h / 20 °C

3.1: acetonitrile / 0.58 h / 150 °C / Microwave irradiation

3.2: 0.17 h / 100 °C / Microwave irradiation

4.1: pyridine / dichloromethane / -10 - 20 °C

With pyridine; hydrogenchloride; DBBA; tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400287v