methyl 5-(p-tolyl)hexanoate

Base Information

Chemical Name:methyl 5-(p-tolyl)hexanoate
CAS No.:73878-68-9
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:220.312
Hs Code.:

Synonyms:methyl 5-(p-tolyl)hexanoate

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Chemical Property of methyl 5-(p-tolyl)hexanoate

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Technology Process of methyl 5-(p-tolyl)hexanoate

There total 5 articles about methyl 5-(p-tolyl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1,3-dioxoisoindolin-2-yl 3-(p-tolyl)butanoate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 73878-68-9
methyl 5-(p-tolyl)hexanoate

Guidance literature:: With nickel(II) perchlorate hexahydrate; lithium chloride; zinc; In acetonitrile; at 25 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.202010840

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 73878-68-9
methyl 5-(p-tolyl)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; potassium tert-butylate; 2-methyl-propan-1-ol / 12 h / 40 °C / Sealed tube

2: dmap; diisopropyl-carbodiimide / dichloromethane / 12 h / 25 °C

3: zinc; nickel(II) perchlorate hexahydrate; lithium chloride / acetonitrile / 12 h / 25 °C / Inert atmosphere; Schlenk technique

With dmap; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; nickel(II) perchlorate hexahydrate; 2-methyl-propan-1-ol; potassium tert-butylate; lithium chloride; diisopropyl-carbodiimide; zinc; In dichloromethane; acetonitrile;
DOI:10.1002/anie.202010840

Reference yield:

: 39027-57-1,58526-36-6
3-(4-methylphenyl)butanoic acid

: 73878-68-9
methyl 5-(p-tolyl)hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; diisopropyl-carbodiimide / dichloromethane / 12 h / 25 °C

2: zinc; nickel(II) perchlorate hexahydrate; lithium chloride / acetonitrile / 12 h / 25 °C / Inert atmosphere; Schlenk technique

With dmap; nickel(II) perchlorate hexahydrate; lithium chloride; diisopropyl-carbodiimide; zinc; In dichloromethane; acetonitrile;
DOI:10.1002/anie.202010840