α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

Base Information

Chemical Name:α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid
CAS No.:175732-28-2
Molecular Formula:C₂₇H₄₃I₃N₆O₄
Molecular Weight:896.39
Hs Code.:

Synonyms:α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

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Chemical Property of α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

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Technology Process of α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

There total 4 articles about α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 160982-41-2
3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

: 175732-28-2
α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

Guidance literature:: In 2,4-dichlorophenoxyacetic acid dimethylamine;

Reference yield: 59.0%

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 160982-41-2
3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

: 175732-28-2
α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

Guidance literature:: With ISOPROPYLAMIDE; at 70 ℃; for 0.5h;

Reference yield:

: 96-83-3
iopanoic acid

: 175732-28-2
α-ethyl-2,4,6-triiodo-3-<<1-oxo-6-<<(1,4,7,10-tetraazacyclododec-1-yl)acetyl>amino>hexyl>amino>benzenepropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH₂Cl₂, 5 deg C, 1 h, 2.) THF, CH₃CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h

2: 59 percent / dimethylacetamide / 0.5 h / 70 °C

With pyridine; oxalyl dichloride; ISOPROPYLAMIDE;