benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside
CAS No.:1251905-57-3
Molecular Formula:C₁₉H₂₉NO₁₀
Molecular Weight:431.44
Hs Code.:

Synonyms:benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

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Chemical Property of benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

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Technology Process of benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

There total 5 articles about benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 50826-96-5
benzyl β-D-galactopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-glucopyranoside

: 1251905-57-3
benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: benzyl β-D-galactopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-glucopyranoside; With potassium hydroxide; at 100 ℃; for 16h;

With hydrogenchloride; In water;
DOI:10.1007/s10719-010-9300-7

Reference yield:

: 1251905-58-4
benzyl (2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl)-(1->6)-2-acetamido-2-deoxy-α-D-glucopyranoside

: 1251905-57-3
benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 2 h / 0 - 20 °C

1.2: Amberlite IR 120 (plus) H+ resin

2.1: potassium hydroxide / 16 h / 100 °C

2.2: Amberlite IR 120 (plus) H+ resin

With sodium methylate; potassium hydroxide; In methanol;
DOI:10.1007/s10719-010-9300-7

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 1251905-57-3
benzyl β-D-galactopyranosyl-(1->6)-2-amino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate / 4 h / 80 °C

2.1: tin(IV) chloride / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: sodium methylate / methanol / 2 h / 0 - 20 °C

3.2: Amberlite IR 120 (plus) H+ resin

4.1: potassium hydroxide / 16 h / 100 °C

4.2: Amberlite IR 120 (plus) H+ resin

With boron trifluoride diethyl etherate; sodium methylate; tin(IV) chloride; potassium hydroxide; In methanol; dichloromethane;
DOI:10.1007/s10719-010-9300-7