tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine

Base Information

• Chemical Name: tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine
• CAS No.: 929601-52-5
• Molecular Formula: C₁₉H₃₀N₂
• Molecular Weight: 286.461

Synonyms:tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine

Chemical Property of tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine

Chemical Property:

Purity/Quality:

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Technology Process of tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine

There total 2 articles about tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-bromo-N-tert-butyl-3,3-dimethyl-N'-(2,4,6-trimethyl-phenyl)-butyramidine (929601-53-6) → tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine (929601-52-5)

Guidance literature:

With potassium tert-butylate; In diethyl ether; at -50 - -15 ℃; for 10.5h;

DOI:10.1021/jo062213y

Reference yield:

2-Bromo-3,3-dimethyl-N-(2,4,6-trimethyl-phenyl)-butyrimidoyl chloride (69959-75-7) → tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine (929601-52-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / tetrahydrofuran / 100 h / Heating

2: 82 percent / potassium tert-butoxide / diethyl ether / 10.5 h / -50 - -15 °C

With potassium tert-butylate; In tetrahydrofuran; diethyl ether;

DOI:10.1021/jo062213y

Reference yield:

tert-butyl-[3-tert-butyl-1-(2,4,6-trimethyl-phenyl)-aziridin-2-ylidene]-amine (929601-52-5) → tert-butylisonitrile (119072-55-8,7188-38-7) + N-(2,2-dimethylpropylidene)-2,4,6-trimethylaniline (208585-37-9)

Guidance literature:

at 0 ℃;

DOI:10.1021/jo062213y

upstream raw materials:

2-bromo-N-tert-butyl-3,3-dimethyl-N'-(2,4,6-trimethyl-phenyl)-butyramidine

2-Bromo-3,3-dimethyl-N-(2,4,6-trimethyl-phenyl)-butyrimidoyl chloride

Downstream raw materials:

tert-butylisonitrile

N-(2,2-dimethylpropylidene)-2,4,6-trimethylaniline

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