-<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt

Base Information

• Chemical Name: -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt
• CAS No.: 141980-80-5
• Molecular Formula: C₃₄H₄₁N₄O₇S*Na
• Molecular Weight: 672.778

Synonyms:-<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt

Chemical Property of -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt

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Technology Process of -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt

There total 2 articles about -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester monosodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

-<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-49-2) → -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester monosodium salt (141980-80-5)

Guidance literature:

With sodium sulfite; In ethanol; for 2h; Heating;

DOI:10.1021/jm00092a007

Reference yield:

tricyclo<3.3.1.13,7>dec-2-yl *,R*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate (130406-64-3) → -<1-(1H-indol-3-ylmethyl)-1-methyl-2-oxo-2-<<2-<(1-oxo-3-sulfopropyl)amino>-2-phenylethyl>amino>ethyl>carbamic acid tricyclo<3.3.1.13,7>dec-2-yl ester monosodium salt (141980-80-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) pentafluorophenol (PFP), N,N'-dicyclohexylcarbodiimide (DCC) / 1.) EtOAc, RT, 2 h, 2.) EtOAc, RT, overnight

2: 52 percent / aq. Na₂SO₃ / aq. ethanol / 2 h / Heating

With 2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; sodium sulfite; In ethanol;

DOI:10.1021/jm00092a007

upstream raw materials:

-<2-<<2-<(3-bromo-1-oxopropyl)amino>-2-phenylethyl>amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

tricyclo<3.3.1.1^3,7>dec-2-yl *,R^*)>-<2-<(2-amino-2-phenylethyl)amino>-1-(1H-indol-3-ylmethyl)-1-methyl-2-oxoethyl>carbamate

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