5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

Base Information

Chemical Name:5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde
CAS No.:670274-96-1
Molecular Formula:C₃₀H₂₆N₂O₉
Molecular Weight:558.544
Hs Code.:

Synonyms:5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

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Chemical Property of 5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

Chemical Property:

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Technology Process of 5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

There total 6 articles about 5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 670274-96-1
5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/ol036300d

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 670274-96-1
5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C

2: sodium borohydride / methanol

3: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C

4: sodium borohydride / methanol

5: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol; 1: Mitsunobu coupling / 3: Mitsunobu coupling / 5: Mitsunobu coupling;
DOI:10.1021/ol036300d

Reference yield:

: 58662-54-7
5-benzyloxy-2-nitrobenzaldehyde

: 670274-96-1
5-[4-(5-benzyloxy-2-nitro-benzyloxy)-3-ethoxy-benzyloxy]-2-nitro-benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: sodium borohydride / methanol

2: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C

3: sodium borohydride / methanol

4: triphenylphosphine; diisopropyl azo-dicarboxylate / tetrahydrofuran / 0 °C

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; methanol; 2: Mitsunobu coupling / 4: Mitsunobu coupling;
DOI:10.1021/ol036300d