C₁₃H₁₄N₂O₃Se

Base Information

Chemical Name:C₁₃H₁₄N₂O₃Se
CAS No.:811438-55-8
Molecular Formula:C₁₃H₁₄N₂O₃Se
Molecular Weight:325.226
Hs Code.:

C<sub>13</sub>H<sub>14</sub>N<sub>2</sub>O<sub>3</sub>Se

Synonyms:C₁₃H₁₄N₂O₃Se

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Chemical Property of C₁₃H₁₄N₂O₃Se

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Technology Process of C₁₃H₁₄N₂O₃Se

There total 8 articles about C₁₃H₁₄N₂O₃Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 811438-53-6
2-phenylselanylmethyl-5,7-diaza-spiro[3.4]octane-6,8-dione

: 811438-55-8
C₁₃H₁₄N₂O₃Se

Guidance literature:: With sodium periodate; In methanol; at 20 ℃; for 24h;
DOI:10.1021/jo048824c

Reference yield:

: 172324-67-3
3-benzyloxymethyl-cyclobutanone

: 811438-55-8
C₁₃H₁₄N₂O₃Se

Guidance literature:: Multi-step reaction with 7 steps

1.1: 97 percent / p-toluenesulfonic acid / benzene / 14 h / 120 °C

2.1: 99 percent / hydrogen / Pd/C / methanol / 24 h / 20 °C

3.1: 94 percent / CBr₄; PPh₃ / CH₂Cl₂ / 6 h / 20 °C

4.1: sodium borohydride / methanol / 20 °C

4.2: 90 percent / methanol / 1.5 h / 20 °C

5.1: 88 percent / HCl / H₂O; ethanol / 19 h / Heating

6.1: 67 percent / H₂O; ethanol / 8 h / 60 °C

7.1: sodium metaperiodate / methanol / 24 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; benzene; 6.1: Buecherer-Strecker reaction;
DOI:10.1021/jo048824c

Reference yield:

: 172324-66-2
3-(benzyloxymethyl)-2,2-dichlorocyclobutanone

: 811438-55-8
C₁₃H₁₄N₂O₃Se

Guidance literature:: Multi-step reaction with 8 steps

1.1: 3.2 g / Zn; acetic acid / 12 h / 120 °C

2.1: 97 percent / p-toluenesulfonic acid / benzene / 14 h / 120 °C

3.1: 99 percent / hydrogen / Pd/C / methanol / 24 h / 20 °C

4.1: 94 percent / CBr₄; PPh₃ / CH₂Cl₂ / 6 h / 20 °C

5.1: sodium borohydride / methanol / 20 °C

5.2: 90 percent / methanol / 1.5 h / 20 °C

6.1: 88 percent / HCl / H₂O; ethanol / 19 h / Heating

7.1: 67 percent / H₂O; ethanol / 8 h / 60 °C

8.1: sodium metaperiodate / methanol / 24 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; acetic acid; triphenylphosphine; zinc; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; benzene; 7.1: Buecherer-Strecker reaction;
DOI:10.1021/jo048824c