4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene

Base Information

• Chemical Name: 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene
• CAS No.: 620598-44-9
• Molecular Formula: C₂₀H₂₅PS₂Si₂
• Molecular Weight: 416.695

Synonyms:4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene

Chemical Property of 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene

Chemical Property:

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Technology Process of 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene

There total 1 articles about 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

Dichlorophenylphosphine (644-97-3) + 3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene (207742-50-5) → 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene (620598-44-9)

Guidance literature:

3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 1h;

Dichlorophenylphosphine; In diethyl ether; hexane; at -30 - 20 ℃;

DOI:10.1002/chem.200500152

Reference yield: 99.0%

4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene (620598-44-9) → 4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene; compound with borane

Guidance literature:

With dimethylsulfide borane complex; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/chem.200500152

Reference yield: 95.0%

4-phenyl-2,6-bis-trimethylsilanyl-4H-phospholo[3,2-b;4,5-b']dithiophene (620598-44-9) → 4-phenyl-2,6-bis-trimethylsilanyl-phospholo[3,2-b;4,5-b']dithiophene 4-oxide

Guidance literature:

With dihydrogen peroxide; In tetrahydrofuran; at 20 ℃;

DOI:10.1002/chem.200500152

upstream raw materials:

Dichlorophenylphosphine

3,3'-dibromo-5,5'-bis(trimethylsilyl)-2,2'-bithiophene

Downstream raw materials:

Rh(C₈H₁₂)Cl(P(C₆H₅)C₈H₂S₂(Si(CH₃)3)2)

W(CO)5(P(C₆H₅)C₈H₂S₂(Si(CH₃)3)2)

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