(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Base Information

Chemical Name:(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide
CAS No.:864948-01-6
Molecular Formula:C₁₃H₁₆N₄O₄
Molecular Weight:292.294
Hs Code.:

Synonyms:(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Suppliers and Price of (3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Chemical Property:

Purity/Quality:

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Technology Process of (3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

There total 8 articles about (3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: methyl (3R,4R,5S)-5-azidomethyl-3,4-dihydroxy-tetrahydrofuran-3-carboxylate

: 100-46-9
benzylamine

: 864948-01-6
(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Guidance literature:: at 120 ℃;
DOI:10.1016/j.tetlet.2005.06.029

Reference yield:

: 5-azido-5-deoxy-2,3-O-isopropylidene-L-lyxose

: 864948-01-6
(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: aq. potassium carbonate

2: aq. bromine; barium carbonate

3: 100 percent / pyridine / CH₂Cl₂

4: 79 percent / hydrogen chloride

5: 95 percent / 120 °C

With pyridine; hydrogenchloride; bromine; potassium carbonate; barium carbonate; In dichloromethane;
DOI:10.1016/j.tetlet.2005.06.029

Reference yield:

: (3aR,6S,6aR)-6-(azidomethyl)-3a-(hydroxymethyl)-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-ol

: 864948-01-6
(3R,4R,5S)-5-Azidomethyl-3,4-dihydroxy-tetrahydro-furan-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 4 steps

1: aq. bromine; barium carbonate

2: 100 percent / pyridine / CH₂Cl₂

3: 79 percent / hydrogen chloride

4: 95 percent / 120 °C

With pyridine; hydrogenchloride; bromine; barium carbonate; In dichloromethane;
DOI:10.1016/j.tetlet.2005.06.029