C₄₇H₄₅N₅O₅Si

Base Information

Chemical Name:C₄₇H₄₅N₅O₅Si
CAS No.:1092804-56-2
Molecular Formula:C₄₇H₄₅N₅O₅Si
Molecular Weight:787.99
Hs Code.:

C<sub>47</sub>H<sub>45</sub>N<sub>5</sub>O<sub>5</sub>Si

Synonyms:C₄₇H₄₅N₅O₅Si

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Chemical Property of C₄₇H₄₅N₅O₅Si

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Technology Process of C₄₇H₄₅N₅O₅Si

There total 12 articles about C₄₇H₄₅N₅O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4005-49-6
N₆-benzoyladenine

: 1092803-02-5
5-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-4-C-(3-propynyl)-α-D-ribofuranose

: 1092804-56-2
C₄₇H₄₅N₅O₅Si

Guidance literature:: 5-O-(tert-butyldiphenylsilyl)-1,2-O-isopropylidene-3-O-(2-naphthylmethyl)-4-C-(3-propynyl)-α-D-ribofuranose; With sulfuric acid; acetic anhydride; acetic acid;

N₆-benzoyladenine; With N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; Reflux;

With ammonia; In methanol;

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1092804-56-2
C₄₇H₄₅N₅O₅Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

6.2: 16.33 h / -78 - 20 °C

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

7.2: 4 h / 50 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.5 h

9.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

9.2: 2 h / -78 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

11.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

13.1: acetic anhydride; sulfuric acid; acetic acid

13.2: Reflux

With sodium periodate; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 13.2: Vorbrugen Reaction;

Reference yield:

: 1091607-89-4
(R)-1-((3aR,5R,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 1092804-56-2
C₄₇H₄₅N₅O₅Si

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium periodate / 1,4-dioxane; water / 1.67 h

2.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

5.2: 16.33 h / -78 - 20 °C

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

6.2: 4 h / 50 °C

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.2: 0.5 h

8.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

8.2: 2 h / -78 °C

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

10.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

11.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

12.1: acetic anhydride; sulfuric acid; acetic acid

12.2: Reflux

With sodium periodate; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 12.2: Vorbrugen Reaction;