C₄₄H₄₈O₁₀

Base Information

• Chemical Name: C₄₄H₄₈O₁₀
• CAS No.: 1449477-38-6
• Molecular Formula: C₄₄H₄₈O₁₀
• Molecular Weight: 736.859
• Mol file: 1449477-38-6.mol

Synonyms:C₄₄H₄₈O₁₀

Chemical Property of C₄₄H₄₈O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₄₈O₁₀

There total 5 articles about C₄₄H₄₈O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H48O7Si → C44H48O10 (1449477-38-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: hydrogen fluoride / acetonitrile; water / 0.25 h / 0 °C

2.1: AD-mix α; methanesulfonamide / water; tert-butyl alcohol / 168 h / 0 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 40 °C / Inert atmosphere

4.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

4.2: 0.42 h / 20 °C / Inert atmosphere; Sonication

5.1: triphenylphosphine; gold(III) chloride; silver trifluoromethanesulfonate / dichloromethane / 7 h / 20 - 50 °C / Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With gold(III) chloride; methanesulfonamide; AD-mix α; di-isopropyl azodicarboxylate; hydrogen fluoride; silver trifluoromethanesulfonate; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol; 2.1: |Sharpless Dihydroxylation;

DOI:10.1002/asia.201201168

Reference yield:

C24H36O9 (1449477-34-2) → C44H48O10 (1449477-38-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 4 h / 0 - 40 °C / Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 0.42 h / 20 °C / Inert atmosphere; Sonication

3.1: triphenylphosphine; gold(III) chloride; silver trifluoromethanesulfonate / dichloromethane / 7 h / 20 - 50 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With gold(III) chloride; di-isopropyl azodicarboxylate; silver trifluoromethanesulfonate; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1002/asia.201201168

Reference yield:

C44H50O10 → C44H48O10 (1449477-38-6)

Guidance literature:

Multi-step reaction with 2 steps

1: triphenylphosphine; gold(III) chloride; silver trifluoromethanesulfonate / dichloromethane / 7 h / 20 - 50 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With gold(III) chloride; silver trifluoromethanesulfonate; Dess-Martin periodane; triphenylphosphine; In dichloromethane;

DOI:10.1002/asia.201201168

upstream raw materials:

C₂₄H₃₆O₉

C₂₄H₃₄O₈

Downstream raw materials:

C₄₄H₅₀O₁₀

C₃₀H₃₈O₁₀

epigallocatechin

Refernces