N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

Base Information

Chemical Name:N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide
CAS No.:214786-46-6
Molecular Formula:C₄₀H₄₃NO₉
Molecular Weight:681.783
Hs Code.:

N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

Synonyms:N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

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Chemical Property of N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

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Technology Process of N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

There total 12 articles about N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25126-93-6
dimethyl trans-3-hexene-1,6-dioate

: 214786-46-6
N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 9 steps

1: 78 percent / LAH / diethyl ether

2: 94 percent / E₃N

3: 84 percent / AD-mix-β

4: 95 percent / H(+)

5: 78 percent / KOH

7: PPh₃, DIAD

8: Cs₂CO₃

9: HCO₂NH₄ / Pd/C

With potassium hydroxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; AD-mix-β; ammonium formate; hydrogen cation; caesium carbonate; triethylamine; triphenylphosphine; palladium on activated charcoal; In diethyl ether;
DOI:10.1016/S0040-4039(98)01468-3

Reference yield:

: N-{2-[3-Benzyloxy-6-(2-{(4R,5R)-5-[2-(7-benzyloxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

: 214786-46-6
N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

Guidance literature:: With ammonium formate; palladium on activated charcoal; Yield given;
DOI:10.1016/S0040-4039(98)01468-3

Reference yield:

: 101357-57-7
(4R)-4r,5t-bis-(2-benzoyloxy-ethyl)-2,2-dimethyl-[1,3]dioxolane

: 214786-46-6
N-{2-[3-Hydroxy-6-(2-{(4R,5R)-5-[2-(7-hydroxy-6-methoxymethoxymethyl-naphthalen-2-yloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-ethoxy)-naphthalen-2-yl]-phenyl}-acetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / KOH

3: PPh₃, DIAD

4: Cs₂CO₃

5: HCO₂NH₄ / Pd/C

With potassium hydroxide; di-isopropyl azodicarboxylate; ammonium formate; caesium carbonate; triphenylphosphine; palladium on activated charcoal;
DOI:10.1016/S0040-4039(98)01468-3