[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

Base Information

Chemical Name:[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde
CAS No.:131026-19-2
Molecular Formula:C₁₇H₂₂O₄
Molecular Weight:290.359
Hs Code.:

Synonyms:[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

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Chemical Property of [(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

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Technology Process of [(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

There total 4 articles about [(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1515-81-7
1-methoxy-4-(methoxymethyl)benzene

: 131026-19-2
[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / DDQ / CH₂Cl₂ / 23 °C

2: 1.) LiAlH₄; 2.) (COCl)2, i-Pr₂NEt / 1.) THF, -12 deg C; 2.) DMSO, CH₂Cl₂, -78 deg C

With lithium aluminium tetrahydride; oxalyl dichloride; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1016/S0040-4039(00)97711-6

Reference yield:

: 131049-58-6
(3R,5R)-3,5-Dihydroxy-7-methyl-oct-6-enoic acid ethyl ester

: 131026-19-2
[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / DDQ / CH₂Cl₂ / 23 °C

2: 1.) LiAlH₄; 2.) (COCl)2, i-Pr₂NEt / 1.) THF, -12 deg C; 2.) DMSO, CH₂Cl₂, -78 deg C

With lithium aluminium tetrahydride; oxalyl dichloride; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1016/S0040-4039(00)97711-6

Reference yield:

: 131049-57-5
(R)-5-Hydroxy-7-methyl-3-oxo-oct-6-enoic acid ethyl ester

: 131026-19-2
[(4R,6R)-2-(4-Methoxy-phenyl)-6-(2-methyl-propenyl)-[1,3]dioxan-4-yl]-acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / Me₄NBH(OAc)3 / acetonitrile; acetic acid / -40 °C

2: 75 percent / DDQ / CH₂Cl₂ / 23 °C

3: 1.) LiAlH₄; 2.) (COCl)2, i-Pr₂NEt / 1.) THF, -12 deg C; 2.) DMSO, CH₂Cl₂, -78 deg C

With lithium aluminium tetrahydride; oxalyl dichloride; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride; In dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/S0040-4039(00)97711-6