C₁₆H₂₃NOS

Base Information

Chemical Name:C₁₆H₂₃NOS
CAS No.:1361202-65-4
Molecular Formula:C₁₆H₂₃NOS
Molecular Weight:277.431
Hs Code.:

Synonyms:C₁₆H₂₃NOS

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Chemical Property of C₁₆H₂₃NOS

Chemical Property:

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Technology Process of C₁₆H₂₃NOS

There total 4 articles about C₁₆H₂₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1361202-90-5
C₁₆H₂₅NOS

: 1361202-65-4
C₁₆H₂₃NOS

Guidance literature:: With palladium(II) trifluoroacetate; lithium acetate; oxygen; In dimethyl sulfoxide; at 50 ℃; for 24h; under 760.051 Torr; optical yield given as %de; diastereoselective reaction; Molecular sieve;
DOI:10.1021/ol3000519

Reference yield:

: 4634-89-3
cis-hex-4-enal

: 1361202-65-4
C₁₆H₂₃NOS

Guidance literature:: Multi-step reaction with 3 steps

1.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: dichloromethane / -50 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: palladium(II) trifluoroacetate; lithium acetate; oxygen / dimethyl sulfoxide / 24 h / 50 °C / 760.05 Torr / Molecular sieve

With titanium(IV) tetraethanolate; palladium(II) trifluoroacetate; lithium acetate; oxygen; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 3.1: Wacker type oxidative cyclization;
DOI:10.1021/ol3000519

Reference yield:

: 928-91-6
(Z)-4-hexenol

: 1361202-65-4
C₁₆H₂₃NOS

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-methyl-1H-imidazole; [2,2]bipyridinyl; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen / acetonitrile / 20 °C

2.1: titanium(IV) tetraethanolate / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: dichloromethane / -50 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: palladium(II) trifluoroacetate; lithium acetate; oxygen / dimethyl sulfoxide / 24 h / 50 °C / 760.05 Torr / Molecular sieve

With 1-methyl-1H-imidazole; [2,2]bipyridinyl; titanium(IV) tetraethanolate; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium(II) trifluoroacetate; lithium acetate; oxygen; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; 4.1: Wacker type oxidative cyclization;
DOI:10.1021/ol3000519