5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

Base Information

Chemical Name:5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide
CAS No.:1314801-60-9
Molecular Formula:C₄₄H₄₅NO₆
Molecular Weight:683.844
Hs Code.:

Synonyms:5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

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Chemical Property of 5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

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Technology Process of 5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

There total 2 articles about 5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1314801-58-5
5-(anthracen-9-yloxy)-N-((2S,3S)-1,3-dihydroxybutan-2-yl)pentanamide

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1314801-60-9
5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

Guidance literature:: With pyridine; dmap; at 20 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1039/c1cc11205h

Reference yield:

: 913627-86-8
5-(anthracen-9-yloxy)pentanoic acid

: 1314801-60-9
5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere; Darkness

1.2: 40 h / 40 °C / Inert atmosphere

2.1: pyridine; dmap / 24 h / 20 °C / Inert atmosphere; Darkness

With pyridine; dmap; benzotriazol-1-ol; diisopropyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1039/c1cc11205h

Reference yield: 59.0%

: 1314801-60-9
5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1314801-62-1
(2S,3S)-3-(5-(anthracen-9-yloxy)pentanamido)-4-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-yl (2-cyanoethyl) diisopropylphosphoramidite

Guidance literature:: 5-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)pentanamide; 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Darkness;

In dichloromethane; for 1h; Inert atmosphere; Darkness;
DOI:10.1039/c1cc11205h