(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

Base Information

Chemical Name:(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal
CAS No.:346611-16-3
Molecular Formula:C₂₇H₃₃NO₂
Molecular Weight:403.565
Hs Code.:

Synonyms:(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

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Chemical Property of (S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

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Technology Process of (S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

There total 5 articles about (S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123054-12-6,123808-74-2,136370-73-5,111060-64-1
(2S)-N,N-dibenzylphenylalaninal

: 122-51-0
orthoformic acid triethyl ester

: 346611-16-3
(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

Guidance literature:: With sulfuric acid; In ethanol;
DOI:10.1016/S0040-4039(01)00292-1

Reference yield:

: 111060-52-7
(S)-2-(dibenzylamino)-3-phenylpropan-1-ol

: 346611-16-3
(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 3.5 h / -61 - 20 °C

2: 7.11 g / HCl; H₂SO₄ / diethyl ether; ethanol / 48 h / 20 °C

With hydrogenchloride; oxalyl dichloride; sulfuric acid; dimethyl sulfoxide; triethylamine; In diethyl ether; ethanol; dichloromethane; 1: Swern oxidation;
DOI:10.1039/b210116e

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 346611-16-3
(S)-2-(N,N-dibenzyl)amino-3-phenylpropanal diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: KI / dimethylformamide / 80 °C

3: H₂SO₄ / ethanol

With sulfuric acid; potassium iodide; In ethanol; N,N-dimethyl-formamide; 2: Swern oxidation;
DOI:10.1016/S0040-4039(01)00292-1