N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

Base Information

Chemical Name:N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine
CAS No.:1254961-57-3
Molecular Formula:C₃₃H₃₁NO₂S
Molecular Weight:505.681
Hs Code.:

Synonyms:N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

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Chemical Property of N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

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Technology Process of N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

There total 6 articles about N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: N-(4-iodophenyl)-N-phenylnaphthalen-1-amine

: 1254961-62-0
2-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1254961-57-3
N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; at 110 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c0jm00854k

Reference yield:

: 14282-76-9
2-bromo-3-methylthiophene

: 1254961-57-3
N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 6 h / 70 °C

2.1: toluene-4-sulfonic acid / benzene / 3 h / Reflux

3.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 16 h / 110 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; potassium carbonate; toluene-4-sulfonic acid; trichlorophosphate; In tetrahydrofuran; hexane; water; toluene; benzene; 4.1: Suzuki coupling;
DOI:10.1039/c0jm00854k

Reference yield:

: 90-30-2
N-phenyl-1-naphthylamine

: 1254961-57-3
N-(4-(5-(5,5-dimethyl-1,3-dioxan-2-yl)-3-methylthiophen-2-yl)phenyl)-N-phenylnaphthalen-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 18-crown-6 ether; copper; potassium carbonate / 1,2-dichloro-benzene / 20 h / 180 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; toluene / 16 h / 110 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 18-crown-6 ether; copper; potassium carbonate; In water; 1,2-dichloro-benzene; toluene; 1: Ullmann reaction / 2: Suzuki coupling;
DOI:10.1039/c0jm00854k