1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

Base Information

Chemical Name:1-chloro-1-(2-furyl)-3-phenyl-2-azapropene
CAS No.:6436-35-7
Molecular Formula:C₁₂H₁₀ClNO
Molecular Weight:219.671
Hs Code.:

Synonyms:1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

Suppliers and Price of 1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

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Technology Process of 1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

There total 2 articles about 1-chloro-1-(2-furyl)-3-phenyl-2-azapropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 10354-48-0
furan-2-carboxylic acid benzylamide

: 6436-35-7
1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

Guidance literature:: With thionyl chloride; at 75 - 80 ℃;

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 100-46-9
benzylamine

: 6436-35-7
1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C / Schlenk technique

2: phosphorus pentachloride / dichloromethane / 1 h / 20 °C / Schlenk technique

With phosphorus pentachloride; In dichloromethane;
DOI:10.1039/c4dt00372a

Reference yield:

: 6436-35-7
1-chloro-1-(2-furyl)-3-phenyl-2-azapropene

: 62-53-3
aniline

: 6436-38-0
N-benzyl-N'-phenylfuran-2-carboximidamide

Guidance literature:: aniline; With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;

1-chloro-1-(2-furyl)-3-phenyl-2-azapropene; In dichloromethane; at 0 - 50 ℃; for 2h;
DOI:10.1021/ol500864r