tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate

Base Information

• Chemical Name: tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate
• CAS No.: 219720-26-0
• Molecular Formula: C₇₉H₁₉NO₂
• Molecular Weight: 1014.03

Synonyms:tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate

Chemical Property of tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate

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Technology Process of tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate

There total 1 articles about tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-(diphenylmethylene)glycine tert-butyl ester (81477-94-3) + fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) → tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate (219720-26-0)

Guidance literature:

With carbon tetrabromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In chlorobenzene; Ambient temperature;

DOI:10.1039/a806865h

Reference yield: 44.0%

tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate (219720-26-0) → tert-butyl 1,2-dihydro-α-diphenylmethylamino[60]fullerenylacetate

Guidance literature:

With sodium cyanoborohydride; In tetrahydrofuran; methanol;

DOI:10.1039/a806865h

Reference yield: 39.0%

tert-butyl 61-diphenylmethylideneamino-1,2-methano[60]fullerene-61-carboxylate (219720-26-0) → fullerene-C60 (99685-96-8,161105-99-3,161106-00-9,111138-12-6,133318-63-5,134053-11-5,134931-35-4,134931-36-5,139703-76-7,145633-27-8,175414-73-0,175414-74-1,175414-75-2,175519-12-7,175519-13-8,175519-14-9,175519-15-0,136376-46-0,144906-37-6,144906-38-7,151767-00-9,152882-97-8,152882-98-9,152882-99-0,153062-34-1,154171-74-1,154171-75-2,154333-99-0,154334-00-6,154397-63-4,154460-59-0,199456-56-9,108739-25-9,120329-57-9,120329-58-0) + tert-butyl 1,2-dihydro-α-diphenylmethylamino[60]fullerenylacetate

Guidance literature:

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; at 20 ℃; for 2h; pH=4.0;

DOI:10.1021/jo025928j

upstream raw materials:

N-(diphenylmethylene)glycine tert-butyl ester

fullerene-C₆₀

Downstream raw materials:

fullerene-C₆₀

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