1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

Base Information

Chemical Name:1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole
CAS No.:1547449-75-1
Molecular Formula:C₂₅H₃₈NO₂
Molecular Weight:384.582
Hs Code.:

Synonyms:1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

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Chemical Property of 1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

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Technology Process of 1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

There total 2 articles about 1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₅₂NO₂Si

: 1547449-75-1
1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; water; at 20 ℃; for 0.25h;
DOI:10.1007/s00706-013-1144-y

Reference yield:

: 2,5-Dihydro-3-formyl-4-hydroxymethyl-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxyl radical

: 1547449-75-1
1-oxyl-3-hydroxymethyl-2,2,5,5-tetramethyl-4-[(1E,3E,5E)-4-methyl-6-(2,6,6-trimethylcyclohex-1-en-1-yl)hexa-1,3,5-trien-1-yl]-2,5-dihydro-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 0 - 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.25 h / -78 °C

2.2: 2 h / -78 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.25 h / 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; water; N,N-dimethyl-formamide;
DOI:10.1007/s00706-013-1144-y