[3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine

Base Information

• Chemical Name: [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine
• CAS No.: 49656-93-1
• Molecular Formula: C₁₇H₁₇N₅O₂S
• Molecular Weight: 355.42
• Mol file: 49656-93-1.mol

Synonyms:[3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine

Chemical Property of [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine

There total 3 articles about [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

ethyl [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetate (131142-17-1) → [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine (49656-93-1)

Guidance literature:

With hydrazine; In ethanol; for 4h; Heating;

Reference yield:

2-[3-phenoxymethyl-4-phenyl-1,2,4-triazole]-5-thiol (21358-13-4) → [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine (49656-93-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / sodium hydroxide / ethanol / 0.17 h / Heating

2: 92 percent / hydrazine / ethanol / 4 h / Heating

With sodium hydroxide; hydrazine; In ethanol;

Reference yield:

→ [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetylhydrazine (49656-93-1)

Guidance literature:

4-Phenyl-1,2,4-triazol-3-mercaptomethylacetat (IIIc), Hydrazinhydrat/Methanol;

upstream raw materials:

ethyl [3-phenoxymethyl-4-phenyl-1,2,4-triazole-5-yl-thio]acetate

2-[3-phenoxymethyl-4-phenyl-1,2,4-triazole]-5-thiol

Downstream raw materials:

(5-Phenoxymethyl-4-phenyl-4H-[1,2,4]triazol-3-ylsulfanyl)-acetic acid [1-(4-nitro-phenyl)-meth-(Z)-ylidene]-hydrazide

(5-Phenoxymethyl-4-phenyl-4H-[1,2,4]triazol-3-ylsulfanyl)-acetic acid [1-phenyl-meth-(Z)-ylidene]-hydrazide

(5-Phenoxymethyl-4-phenyl-4H-[1,2,4]triazol-3-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(Z)-ylidene]-hydrazide

(5-Phenoxymethyl-4-phenyl-4H-[1,2,4]triazol-3-ylsulfanyl)-acetic acid [1-(2-hydroxy-phenyl)-meth-(Z)-ylidene]-hydrazide