1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

Base Information

Chemical Name:1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride
CAS No.:1202027-91-5
Molecular Formula:C₂₅H₃₅N₂*Cl
Molecular Weight:399.019
Hs Code.:

Synonyms:1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

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Technology Process of 1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

There total 1 articles about 1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1202027-87-9
N-(2,3,4,5,6-pentamethylbenzyl)imidazoline

: 1585-16-6
2-chloromethyl-1,3,5-trimethylbenzene

: 1202027-91-5
1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 70 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.08.030

Reference yield: 87.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1202027-91-5
1-(2,3,4,5,6-pentamethylbenzyl)-3-(2,4,6-trimethylbenzyl)imidazolinium chloride

: RuCl2[η1-CN(CH2(η6-C6(CH3)5-2,3,4,5,6))CH2CH2N(CH2C6H2(CH3)3-2,4,6)]

Guidance literature:: With caesium carbonate; In toluene; under Ar; suspension of imidazolium salt (2.1 mmol), Cs2CO3 (2.14 mmol),and (RuCl2(p-cymene))2 (0.82 mmol) refluxed in degassed toluene for 6 h; filtered while hot, concd., n-hexane added, ppt. recrystd. (CH2Cl2/hexane 1:3 v:v); elem. anal.;
DOI:10.1016/j.jorganchem.2009.08.030