Technology Process of (biphenylyl-4)-6 methyl-4 dihydro-4,5 pyridazine (2-H) one-3
There total 6 articles about (biphenylyl-4)-6 methyl-4 dihydro-4,5 pyridazine (2-H) one-3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 60 percent / anhydr. aluminum chloride / nitrobenzene / 4 h / Ambient temperature
2: 95 percent / 85percent hydrazine hydrate / 2-methoxy-ethanol / 2 h / Heating
With
aluminium trichloride; hydrazine hydrate;
In
2-methoxy-ethanol; nitrobenzene;
DOI:10.1016/0223-5234(87)90173-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / anhydr. aluminum chloride / nitrobenzene / 4 h / Ambient temperature
2: 88 percent / hydrogen / 10percent palladium-on-carbon / dimethylformamide
3: 95 percent / 85percent hydrazine hydrate / 2-methoxy-ethanol / 2 h / Heating
With
aluminium trichloride; hydrogen; hydrazine hydrate;
palladium on activated charcoal;
In
2-methoxy-ethanol; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(87)90173-5
