3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

Base Information

Chemical Name:3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide
CAS No.:1354917-06-8
Molecular Formula:C₁₆H₁₂N₄O₃S₃
Molecular Weight:404.494
Hs Code.:

Synonyms:3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

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Technology Process of 3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

There total 3 articles about 3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1354917-73-9
3-cyano-N-(2,4-dimethoxybenzyl)-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

: 1354917-06-8
3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃;

Reference yield:

: 1235406-41-3
3-cyano-N-[(2,4-dimethoxyphenyl)methyl]-4-fluoro-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

: 1354917-06-8
3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dimethyl sulfoxide / 50 °C

2: hydrogenchloride / 1,4-dioxane / 20 °C

With hydrogenchloride; potassium carbonate; In 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

: 351003-23-1
3-cyano-4-fluorobenzene-1-sulfonyl chloride

: 1354917-06-8
3-cyano-4-[(3-methoxyphenyl)thio]-N-1,2,4-thiadiazol-5-ylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium bis(trimethylsilyl)azanide / tetrahydrofuran / 2.08 h / -78 - 78 °C / Inert atmosphere

1.2: -78 - 20 °C

2.1: potassium carbonate / dimethyl sulfoxide / 50 °C

3.1: hydrogenchloride / 1,4-dioxane / 20 °C

With hydrogenchloride; lithium bis(trimethylsilyl)azanide; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide;