C₂₀H₂₈IN₃O₄

Base Information

Chemical Name:C₂₀H₂₈IN₃O₄
CAS No.:946063-37-2
Molecular Formula:C₂₀H₂₈IN₃O₄
Molecular Weight:501.365
Hs Code.:

C<sub>20</sub>H<sub>28</sub>IN<sub>3</sub>O<sub>4</sub>

Synonyms:C₂₀H₂₈IN₃O₄

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Chemical Property of C₂₀H₂₈IN₃O₄

Chemical Property:

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Technology Process of C₂₀H₂₈IN₃O₄

There total 10 articles about C₂₀H₂₈IN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 946063-36-1
C₂₀H₂₉N₃O₅

: 946063-37-2
C₂₀H₂₈IN₃O₄

Guidance literature:: With 1H-imidazole; iodine; thiamine diphosphate; In toluene; acetonitrile;
DOI:10.1016/j.tetlet.2007.05.079

Reference yield:

: 946063-31-6
(3aS,4S,6R,6aR)-4-((4-methoxybenzyl)oxy)-2,2-dimethyl-6-vinyltetrahydro-3aH-cyclopenta[d][1,3]dioxole

: 946063-37-2
C₂₀H₂₈IN₃O₄

Guidance literature:: Multi-step reaction with 8 steps

1.1: 9-BBN / tetrahydrofuran

1.2: 98 percent / H₂O₂; NaOH / methanol

2.1: 94 percent / SO₃*py; DMSO; DIPEA / CH₂Cl₂

3.1: (+)-B-methoxydiisopinocampheylborane / diethyl ether; tetrahydrofuran

3.2: 96 percent / H₂O₂; NaOH / methanol

4.1: Et₃N; DMAP / CH₂Cl₂

5.1: NaN₃ / dimethylformamide

6.1: NaIO₄; OsO₄ / methanol; H₂O

7.1: NaBH₄; CeCl₃*7H₂O / methanol

8.1: 90 percent / TPP; imidazole; I₂ / toluene; acetonitrile

With (+)-Ipc₂BOMe; 1H-imidazole; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; 9-borabicyclo[3.3.1]nonane dimer; sodium azide; cerium(III) chloride; pyridine-SO₃ complex; iodine; thiamine diphosphate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Brown allylboration / 7.1: Luche reduction;
DOI:10.1016/j.tetlet.2007.05.079

Reference yield:

: C₂₀H₂₇N₃O₅

: 946063-37-2
C₂₀H₂₈IN₃O₄

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄; CeCl₃*7H₂O / methanol

2: 90 percent / TPP; imidazole; I₂ / toluene; acetonitrile

With 1H-imidazole; sodium tetrahydroborate; cerium(III) chloride; iodine; thiamine diphosphate; In methanol; toluene; acetonitrile; 1: Luche reduction;
DOI:10.1016/j.tetlet.2007.05.079