(+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL

Base Information

• Chemical Name: (+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL
• CAS No.: 86436-19-3
• Molecular Formula: C30H20 Cl2 O2
• Molecular Weight: 483.394
• Hs Code.: 2906299090
• Mol file: 86436-19-3.mol

Synonyms:(+)-1,6-Diphenyl-1,6-di(o-chlorophenyl)-2,4-hexadiyne-1,6-diol

Chemical Property of (+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL

Chemical Property:

• Melting Point: 130-133 °C
• Refractive Index: 1.4730 (estimate)
• Boiling Point: 584.23°C (rough estimate)
• PSA: 40.46000
• Density: 1.1012 (rough estimate)
• LogP: 6.17220
• Storage Temp.: 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

(+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL 95.00% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL

There total 1 articles about (+)-1,6-BIS(2-CHLOROPHENYL)-1,6-DIPHENYL-2,4-HEXADIYNE-1,6-DIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,6-bis(o-chlorophenyl)1,6-diphenylhexa-2,4-diyne-1,6-diol-N,N-dimethyl-α-oxobenzeneacetamide (115118-99-5) → (S,S)(-)-1,6-bis-(o-chlorophenyl)-1,6-diphenylhexa-2,4-diyne-1,6-diol (86436-19-3) + (S)-(-)-1-methyl-3-phenyl-3-hydroxyazetidin-2-one (115119-00-1)

Guidance literature:

for 27h; Ambient temperature; Irradiation;

DOI:10.1021/jo00253a037

Reference yield: 97.0%

2-ethyltropolone (61697-22-1) + (S,S)(-)-1,6-bis-(o-chlorophenyl)-1,6-diphenylhexa-2,4-diyne-1,6-diol (86436-19-3) → (S)-(-)-6-bis(o-chlorophenyl)-1,6-diphenylhexa-2,4-diyne-1,6-diol-tropolone ethyl ether (107932-02-5)

Guidance literature:

In hexane; benzene; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90265-0

Reference yield: 97.0%

2-hydroxy-2,4,6-cycloheptatrien-1-one (533-75-5) + (S,S)(-)-1,6-bis-(o-chlorophenyl)-1,6-diphenylhexa-2,4-diyne-1,6-diol (86436-19-3) → (1R,6R)-1,6-Bis-(2-chloro-phenyl)-1,6-diphenyl-hexa-2,4-diyne-1,6-diol; compound with 2-hydroxy-cyclohepta-2,4,6-trienone (113397-22-1)

Guidance literature:

In hexane; benzene; for 12h; Ambient temperature;

DOI:10.1016/S0040-4020(01)90265-0

upstream raw materials:

1,6-bis(o-chlorophenyl)1,6-diphenylhexa-2,4-diyne-1,6-diol-N,N-dimethyl-α-oxobenzeneacetamide

Downstream raw materials:

1,6-Bis-(2-chloro-phenyl)-1,6-diphenyl-hexa-2,4-diyne-1,6-diol; compound with bicyclo[5.1.0]octa-3,5-dien-2-one

1,6-Bis-(2-chloro-phenyl)-1,6-diphenyl-hexa-2,4-diyne-1,6-diol; compound with (2Z,4Z)-cycloocta-2,4-dienone

1α,2α,4α,6α-Tricyclo[4.2.0.0^2,4]oct-7-en-5-on

C₃₀H₂₀Cl₂O₂*C₆H₁₅NOS

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