Technology Process of MeO-Ser(Bzl)-bromoketal
There total 2 articles about MeO-Ser(Bzl)-bromoketal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
for 3h;
Inert atmosphere;
DOI:10.1021/ol203290n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diazomethyl-trimethyl-silane / benzene / Inert atmosphere
2: methoxybenzene; trifluoroacetic acid / dichloromethane / Inert atmosphere
3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
With
O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; methoxybenzene; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; diazomethyl-trimethyl-silane;
In
dichloromethane; benzene;
DOI:10.1016/j.tetlet.2014.10.089
