Technology Process of H2dipic
There total 4 articles about H2dipic which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C38H44N2O8;
With
sodium hydroxide;
In
tetrahydrofuran; ethanol; water;
at 60 ℃;
for 2h;
With
water;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tet.2011.01.042
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid; benzene / 24 h / Inert atmosphere; Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere
3: potassium acetate / N,N-dimethyl-formamide / 24 h / Inert atmosphere; Reflux
4: sodium hydroxide / tetrahydrofuran; ethanol; water / 2 h / 60 °C
With
sulfuric acid; potassium acetate; potassium carbonate; sodium hydroxide; benzene;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
3: Williamson synthesis;
DOI:10.1016/j.tet.2011.01.042
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere
2: potassium acetate / N,N-dimethyl-formamide / 24 h / Inert atmosphere; Reflux
3: sodium hydroxide / tetrahydrofuran; ethanol; water / 2 h / 60 °C
With
potassium acetate; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
2: Williamson synthesis;
DOI:10.1016/j.tet.2011.01.042
