2-(perfluorophenyl)benzo[b]thiophene

Base Information

• Chemical Name: 2-(perfluorophenyl)benzo[b]thiophene
• CAS No.: 38210-37-6
• Molecular Formula: C₁₄H₅F₅S
• Molecular Weight: 300.252

Synonyms:2-(perfluorophenyl)benzo[b]thiophene

Chemical Property of 2-(perfluorophenyl)benzo[b]thiophene

Chemical Property:

Purity/Quality:

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Technology Process of 2-(perfluorophenyl)benzo[b]thiophene

There total 3 articles about 2-(perfluorophenyl)benzo[b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Pentafluorobenzene (363-72-4) + Benzo[b]thiophene (95-15-8,11095-43-5) → 2-(perfluorophenyl)benzo[b]thiophene (38210-37-6)

Guidance literature:

With oxygen; palladium diacetate; silver(l) oxide; Trimethylacetic acid; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 120 ℃; for 9h; under 760.051 Torr; Mechanism; Autoclave;

DOI:10.1021/om200873j

Reference yield:

Pentafluorobenzene (363-72-4) + Benzo[b]thiophene (95-15-8,11095-43-5) → 3-(perfluorophenyl)benzo[b]thiophene (38210-39-8) + 2-(perfluorophenyl)benzo[b]thiophene (38210-37-6)

Guidance literature:

With (triphenylphosphine)gold(I) chloride; 1-pivaloyloxy-1,2-benziodoxol-3(1H)-one; silver pivalate; dimethyl sulfoxide; In 1,4-dioxane; at 110 ℃; for 16h; Overall yield = 75 %; Overall yield = 45 mg; regioselective reaction; Inert atmosphere;

DOI:10.1021/jacs.5b10593

Reference yield:

→ 2-(perfluorophenyl)benzo[b]thiophene (38210-37-6)

Guidance literature:

2-Benzothienyllithium, Hexafluorbenzol;

DOI:10.1039/P19720002023

upstream raw materials:

Pentafluorobenzene

Benzo[b]thiophene

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