anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone

Base Information

• Chemical Name: anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone
• CAS No.: 140438-54-6
• Molecular Formula: C₂₄H₂₀N₆O₄
• Molecular Weight: 456.461

Synonyms:anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone

Chemical Property of anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone

There total 1 articles about anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadecane-4,6,13,15-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.11,9.02,8.03,7.012,16>octadec-9-ene-4,6,13,15-tetraone (140438-53-5) → anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.11,9.02,8.03,7.012,16>octadecane-4,6,13,15-tetraone (140438-54-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 120h;

Reference yield:

anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.11,9.02,8.03,7.012,16>octadecane-4,6,13,15-tetraone (140438-54-6) → 3,4,9,10-tetraazatetracyclo<6.2.1.11,6.02,5>dodeca-3,9-diene (140438-57-9)

Guidance literature:

With potassium hydroxide; ammonium hydroxide; copper dichloride; Yield given. Multistep reaction; 1.) isopropyl alcohol, reflux, 15 h, 2.) isopropyl alcohol, water, 15 min;

Reference yield:

anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.11,9.02,8.03,7.012,16>octadecane-4,6,13,15-tetraone (140438-54-6) → 3,4-diazatetracyclo<6.1.12,5.02,7.0>dec-3-ene (140438-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) KOH, 2.) CuCl₂, aq. NH₃ / 1.) isopropyl alcohol, reflux, 15 h, 2.) isopropyl alcohol, water, 15 min

2: CH₂Cl₂ / 0.05 h / 0 °C / Irradiation

With potassium hydroxide; ammonium hydroxide; copper dichloride; In dichloromethane;

upstream raw materials:

anti-3,5,7,12,14,16-hexaaza-5,14-diphenylhexacyclo<9.5.1.1^1,9.0^2,8.0^3,7.0^12,16>octadec-9-ene-4,6,13,15-tetraone

Downstream raw materials:

3,4,9,10-tetraazatetracyclo<6.2.1.1^1,6.0^2,5>dodeca-3,9-diene

3,4-diazatetracyclo<6.1.1^2,5.0^2,7.0>dec-3-ene

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