3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

Base Information

Chemical Name:3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide
CAS No.:1228284-64-7
Molecular Formula:C₁₆H₁₆Cl₃F₂N₃O₂
Molecular Weight:426.678
Hs Code.:

Synonyms:3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

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Chemical Property of 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

Chemical Property:

Melting Point:>96°C (dec.)
Boiling Point:557.9±50.0 °C(Predicted)
Density:1.44±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

Useful:

Uses Pydiflumetofen is used in the preparation of carboxamides as plant growth enhancers in crops.

Technology Process of 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

There total 8 articles about 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

: 141573-96-8
3‐difluoromethyl‐1‐methylpyrazole-4-carbonyl chloride

: 1228284-78-3
O-methyl-N-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-hydroxylamine

: 1228284-64-7
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

Guidance literature:: With triethylamine; In 5,5-dimethyl-1,3-cyclohexadiene; at 70 ℃; for 4h; Temperature; Reagent/catalyst;

Reference yield:

: 1228284-86-3
1-(2,4,6-trichlorophenyl)propan-2-one

: 1228284-64-7
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 3 h / 60 °C

2.1: sodium cyanoborohydride; acetic acid / 6 h / 20 °C

2.2: pH 9

3.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

With sodium cyanoborohydride; acetic acid; triethylamine; In dichloromethane;

Reference yield:

: 1228284-88-5
1,3,5-trichloro-2-((E)-2-nitro-propenyl)-benzene

: 1228284-64-7
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-methyl-2-(2,4,6-trichloro-phenyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; water / methanol / 3 h / 70 °C

2.1: triethylamine / 3 h / 60 °C

3.1: sodium cyanoborohydride; acetic acid / 6 h / 20 °C

3.2: pH 9

4.1: triethylamine / dichloromethane / 18 h / 0 - 20 °C

With hydrogenchloride; water; sodium cyanoborohydride; acetic acid; triethylamine; In methanol; dichloromethane;