phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

Base Information

Chemical Name:phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside
CAS No.:945634-60-6
Molecular Formula:C₂₉H₃₀Cl₃NO₆Se
Molecular Weight:673.879
Hs Code.:

Synonyms:phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

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Chemical Property of phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

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Technology Process of phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

There total 5 articles about phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.9%

: 945634-63-9
phenyl 3,4-di-O-benzyl-6-O-(tert-butyl-dimethyl-silyl)-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

: 945634-60-6
phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; for 0.5h;
DOI:10.1021/jo070629l

Reference yield:

: 945634-62-8
phenyl 2-azido-2-deoxy-3,4-di-O-benzyl-6-O-(tert-butyl-dimethyl-silyl)-1-seleno-α-D-galactopyranoside

: 945634-60-6
phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 1 h / 0 °C

2: 1.12 g / aq. NaHCO₃ / dioxane / 1 h / 20 °C

3: 78.9 percent / p-toluenesulfonic acid monohydrate / methanol; CH₂Cl₂ / 0.5 h

With lithium aluminium tetrahydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; diethyl ether; dichloromethane;
DOI:10.1021/jo070629l

Reference yield:

: C₃₂H₄₃O₄NSeSi

: 945634-60-6
phenyl 3,4-di-O-benzyl-1-seleno-2-deoxy-2-{[(2,2,2-trichloroethoxy)carbonyl]amino}-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.12 g / aq. NaHCO₃ / dioxane / 1 h / 20 °C

2: 78.9 percent / p-toluenesulfonic acid monohydrate / methanol; CH₂Cl₂ / 0.5 h

With sodium hydrogencarbonate; toluene-4-sulfonic acid; In 1,4-dioxane; methanol; dichloromethane;
DOI:10.1021/jo070629l