5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

Base Information

Chemical Name:5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester
CAS No.:795277-24-6
Molecular Formula:C₇₈H₁₂₈I₂O₁₀
Molecular Weight:1479.68
Hs Code.:

Synonyms:5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

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Chemical Property of 5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

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Technology Process of 5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

There total 8 articles about 5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 795277-29-1
5-[4-(4-chlorocarbonyl-butoxy)-2,5-diiodo-phenoxy]-pentanoyl chloride

: 199192-20-6
(3,5-bis(dodecyloxy)phenyl)methanol

: 795277-24-6
5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; dichloromethane; at 40 ℃; for 8h;
DOI:10.1021/ac049163m

Reference yield:

: 795277-28-0
5-[4-(4-carboxybutoxy)-2,5-diiodophenoxy]pentanoic acid

: 795277-24-6
5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride / CH₂Cl₂; dimethylformamide / 6 h / 20 °C

2: 71 percent / pyridine / CH₂Cl₂; tetrahydrofuran / 8 h / 40 °C

With pyridine; oxalyl dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ac049163m

Reference yield:

: 795277-27-9
ethyl 5-{4-[4-(ethoxycarbonyl)butoxy]-2,5-diiodophenoxy}pentanoate

: 795277-24-6
5-{4-[4-(3,5-bis-dodecyloxy-benzyloxycarbonyl)-butoxy]-2,5-diiodo-phenoxy}-pentanoic acid 3,5-bis-dodecyloxy-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 24 h / Heating

2: oxalyl chloride / CH₂Cl₂; dimethylformamide / 6 h / 20 °C

3: 71 percent / pyridine / CH₂Cl₂; tetrahydrofuran / 8 h / 40 °C

With pyridine; potassium hydroxide; oxalyl dichloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ac049163m