2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

Base Information Edit

Chemical Name:2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol
CAS No.:178616-50-7
Molecular Formula:C₁₅H₃₀O₃
Molecular Weight:258.401
Hs Code.:
Mol file:178616-50-7.mol

Synonyms:2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

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Chemical Property of 2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol Edit

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Technology Process of 2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

There total 9 articles about 2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84078-59-1
2-(2'-Methylene-6',6'-dimethylcyclohexyl)ethanol

: 178616-50-7
2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 12 h / 0 - 4 °C

2: NaI / acetone / 4 h / Heating

3: 1.) K₂CO₃, 2.) p-TsOH / 1.) acetone, DMF, 70 deg C, 21 h, 2.) MeOH, 55 deg C, 30 min

4: 78 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature

5: LiAlH₄ / diethyl ether / 2 h / Heating

With pyridine; lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In diethyl ether; dichloromethane; acetone;

Reference yield:

: 76337-18-3
3,3-Dimethylcyclohex-1-ene-1-carbaldehyde

: 178616-50-7
2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

Guidance literature:: Multi-step reaction with 8 steps

1: LiAlH₄ / diethyl ether / 1.) 0 deg C, 20 min, 2.) room temp., 0.5 h

2: 80 percent / propanoic acid / 1 h / 140 - 150 °C

3: 94 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

4: pyridine / 12 h / 0 - 4 °C

5: NaI / acetone / 4 h / Heating

6: 1.) K₂CO₃, 2.) p-TsOH / 1.) acetone, DMF, 70 deg C, 21 h, 2.) MeOH, 55 deg C, 30 min

7: 78 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature

8: LiAlH₄ / diethyl ether / 2 h / Heating

With pyridine; lithium aluminium tetrahydride; potassium carbonate; toluene-4-sulfonic acid; propionic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In diethyl ether; dichloromethane; acetone;

Reference yield:

: 67218-06-8
6-(butylsulfanyl-methylene)-2,2-dimethyl-cyclohexanone

: 178616-50-7
2-[2-(2-Hydroxy-2,6,6-trimethyl-cyclohexyl)-ethyl]-butane-1,3-diol

Guidance literature:: Multi-step reaction with 10 steps

1: NaBH₄ / ethanol; tetrahydrofuran / 1.5 h / 0 °C

2: CdCO₃, HgCl₂ / ethanol / 0.05 h / Heating

3: LiAlH₄ / diethyl ether / 1.) 0 deg C, 20 min, 2.) room temp., 0.5 h

4: 80 percent / propanoic acid / 1 h / 140 - 150 °C

5: 94 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

6: pyridine / 12 h / 0 - 4 °C

7: NaI / acetone / 4 h / Heating

8: 1.) K₂CO₃, 2.) p-TsOH / 1.) acetone, DMF, 70 deg C, 21 h, 2.) MeOH, 55 deg C, 30 min

9: 78 percent / 80percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature

10: LiAlH₄ / diethyl ether / 2 h / Heating

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; cadmium(II) carbonate; potassium carbonate; toluene-4-sulfonic acid; propionic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide; mercury dichloride; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetone;