dimethylcarbamic acid 2-formylphenyl ester

Base Information

• Chemical Name: dimethylcarbamic acid 2-formylphenyl ester
• CAS No.: 21709-45-5
• Molecular Formula: C₁₀H₁₁NO₃
• Molecular Weight: 193.202
• Mol file: 21709-45-5.mol

Synonyms:dimethylcarbamic acid 2-formylphenyl ester

Chemical Property of dimethylcarbamic acid 2-formylphenyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-Formylphenyl dimethylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethylcarbamic acid 2-formylphenyl ester

There total 4 articles about dimethylcarbamic acid 2-formylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N,N-dimethylformamide + salicylaldehyde (90-02-8) → dimethylcarbamic acid 2-formylphenyl ester (21709-45-5)

Guidance literature:

With tert.-butylhydroperoxide; In water; at 70 ℃; for 12h; Reagent/catalyst;

DOI:10.1039/c4dt03236e

Reference yield: 96.0%

salicylaldehyde (90-02-8) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → dimethylcarbamic acid 2-formylphenyl ester (21709-45-5)

Guidance literature:

With tert.-butylhydroperoxide; copper(l) chloride; at 80 ℃; for 0.25h; Reagent/catalyst; Temperature;

DOI:10.1021/jo402798k

Reference yield: 70.0%

salicylaldehyde (90-02-8) + N,N-Dimethylcarbamoyl chloride (79-44-7) → dimethylcarbamic acid 2-formylphenyl ester (21709-45-5)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/bkcs.10626

upstream raw materials:

salicylaldehyde

N,N-dimethyl-formamide

N,N-Dimethylcarbamoyl chloride