[1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine

Base Information

• Chemical Name: [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine
• CAS No.: 118608-44-9
• Molecular Formula: C₁₅H₂₁N₃O₂
• Molecular Weight: 275.351

Synonyms:[1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine

Chemical Property of [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine

Chemical Property:

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Technology Process of [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine

There total 4 articles about [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

4-nitrophenyl azide (1516-60-5) + 4-tert-butyl-3,3-dimethyl-5-methylene-Δ1-1,2,4-triazoline (109853-57-8) → N-tert-Butyl-N'-(4-nitro-phenyl)-acetamidine (118608-46-1) + N-tert-Butyl-N-isopropenyl-N'-(4-nitro-phenyl)-acetamidine (118608-45-0) + [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine (118608-44-9) + tert-Butyl-isopropenyl-[3-(4-nitro-phenyl)-4,5-dihydro-3H-[1,2,3]triazol-4-yl]-amine (118608-47-2)

Guidance literature:

In benzene; at 80 ℃; for 20h; Further byproducts given;

Reference yield:

4-nitrophenyl azide (1516-60-5) + 4-tert-butyl-3,3-dimethyl-5-methylene-Δ1-1,2,4-triazoline (109853-57-8) → 4-nitro-aniline (100-01-6,104810-17-5) + N-tert-Butyl-N'-(4-nitro-phenyl)-acetamidine (118608-46-1) + N-tert-Butyl-N-isopropenyl-N'-(4-nitro-phenyl)-acetamidine (118608-45-0) + [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine (118608-44-9)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) benzene, 80 deg C, 24 h; 2.) toluene, 110 deg C, 12 h;

Reference yield:

9-tert-Butyl-8,8-dimethyl-1-(4-nitro-phenyl)-1,2,3,6,7,9-hexaaza-spiro[4.4]nona-2,6-diene (118608-40-5) → N-tert-Butyl-N'-(4-nitro-phenyl)-acetamidine (118608-46-1) + N-tert-Butyl-N-isopropenyl-N'-(4-nitro-phenyl)-acetamidine (118608-45-0) + [1-tert-Butyl-4,4-dimethyl-azetidin-(2E)-ylidene]-(4-nitro-phenyl)-amine (118608-44-9) + tert-Butyl-isopropenyl-[3-(4-nitro-phenyl)-4,5-dihydro-3H-[1,2,3]triazol-4-yl]-amine (118608-47-2)

Guidance literature:

In benzene; at 80 ℃; for 2h; Further byproducts given;

upstream raw materials:

4-nitrophenyl azide

4-tert-butyl-3,3-dimethyl-5-methylene-Δ¹-1,2,4-triazoline

9-tert-Butyl-8,8-dimethyl-1-(4-nitro-phenyl)-1,2,3,6,7,9-hexaaza-spiro[4.4]nona-2,6-diene

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