N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

Base Information

Chemical Name:N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide
CAS No.:155580-33-9
Molecular Formula:C₄₉H₄₂ClNO₁₂
Molecular Weight:872.325
Hs Code.:

Synonyms:N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

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Chemical Property of N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

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Technology Process of N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

There total 7 articles about N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 155580-29-3
N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-(propenyloxy)phenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

: 155580-33-9
N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: With triethylammonium formate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; for 3h; Heating;
DOI:10.1002/recl.19931121106

Reference yield:

: 128702-23-8,145415-62-9,145415-63-0
(aS)-methyl 2,2'-dihydroxy-1,1'-binaphthalene-3-carboxylate

: 155580-33-9
N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / K₂CO₃ / acetonitrile / Heating

2: p-toluenesulfonic acid, 3 Angstroem molecular sieves / CHCl₃ / 2 h / Heating

3: aq. KOH / methanol / 2 h / Heating

4: 1.) HOBT*H₂O, DCC / 1.) CH₂Cl₂, 1 h, 2.) overnight

5: 1 N aq. HCl / tetrahydrofuran / 1 h

6: 100 percent / HCOONHEt₃ / Pd(PPh₃)4 / tetrahydrofuran; aq. ethanol / 3 h / Heating

With hydrogenchloride; potassium hydroxide; 3 A molecular sieve; triethylammonium formate; potassium carbonate; benzotriazol-1-ol; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; chloroform; acetonitrile;
DOI:10.1002/recl.19931121106

Reference yield:

: 152523-73-4
3-<2-(2-hydroxyethoxy)ethoxy>-2-(2-propenyloxy)benzaldehyde 4-methylbenzenesulfonate

: 155580-33-9
N-(5-Chloro-2-hydroxyphenyl)-2,2'-bis<2-<2-<3-formyl-2-hydroxyphenoxy>ethoxy>ethoxy>-<1,1'-binaphthalene>-3-carboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / K₂CO₃ / acetonitrile / Heating

2: p-toluenesulfonic acid, 3 Angstroem molecular sieves / CHCl₃ / 2 h / Heating

3: aq. KOH / methanol / 2 h / Heating

4: 1.) HOBT*H₂O, DCC / 1.) CH₂Cl₂, 1 h, 2.) overnight

5: 1 N aq. HCl / tetrahydrofuran / 1 h

6: 100 percent / HCOONHEt₃ / Pd(PPh₃)4 / tetrahydrofuran; aq. ethanol / 3 h / Heating

With hydrogenchloride; potassium hydroxide; 3 A molecular sieve; triethylammonium formate; potassium carbonate; benzotriazol-1-ol; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; chloroform; acetonitrile;
DOI:10.1002/recl.19931121106