2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-

Base Information

Chemical Name:2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-
CAS No.:82013-34-1
Molecular Formula:C₁₄H₁₃Cl₂N₃O
Molecular Weight:310.183
Hs Code.:
Mol file:82013-34-1.mol

Synonyms:2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-

Suppliers and Price of 2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of 2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)-

There total 2 articles about 2-Propen-1-one, 1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-(1H-imidazol-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4252-78-2
2,2',4'-trichloroacetophenone

: 82013-34-1
1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-imidazolylprop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2.25 h / 75 °C

2: 9 h / 105 °C

In toluene;
DOI:10.1021/acs.jmedchem.7b00922

Reference yield:

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 46503-52-0
1-(2,4-dichlorophenyl)-2-(imidazol-1-yl)ethanone

: 82013-34-1
1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-imidazolylprop-2-en-1-one

Guidance literature:: at 105 ℃; for 9h;
DOI:10.1021/acs.jmedchem.7b00922

Reference yield:

: 82013-34-1
1-(2,4-dichlorophenyl)-3-(dimethylamino)-2-imidazolylprop-2-en-1-one

: 252917-24-1
{6-[(2-{[4-(2,4-dichlorophenyl)-5-imidazolylpyrimidin-2-yl]amino}ethyl)amino]-3-nitro(2-pyridyl)}dimethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / 1-methyl-pyrrolidin-2-one / 48 h / 100 °C

2: hydrogenchloride / acetonitrile; water / 16 h / 25 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 80 °C

With hydrogenchloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.jmedchem.7b00922