2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

Base Information

Chemical Name:2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose
CAS No.:141266-01-5
Molecular Formula:C₃₈H₅₃N₅O₁₂
Molecular Weight:771.865
Hs Code.:

2-<N-<N-(N,N'-dicarbobenzyloxy)-L-lysyl>-L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

Synonyms:2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

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Chemical Property of 2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

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Technology Process of 2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

There total 3 articles about 2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 141280-21-9
2--L-valyl>-L-prolylamido-2-deoxy-1,3,4,6-tetra-O-acetyl-β-D-glucose

: 141266-01-5
2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol; at -10 - 20 ℃; for 0.5h;
DOI:10.1016/0223-5234(91)90001-4

Reference yield:

: 5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5
1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride

: 141266-01-5
2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) i-BuOCOCl, N-methylmorpholine, 2.) N-methylmorpholine / 1.) THF, -15 deg C, 30 min, 2.) THF, 4 deg C, 15 h

2: 71 percent / NaOMe / tetrahydrofuran; methanol / 0.5 h / -10 - 20 °C

With 4-methyl-morpholine; sodium methylate; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1016/0223-5234(91)90001-4

Reference yield:

: 95500-87-1
-L-valyl>-L-proline

: 141266-01-5
2--L-valyl>-L-prolylamido-2-deoxy-β-D-glucose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) i-BuOCOCl, N-methylmorpholine, 2.) N-methylmorpholine / 1.) THF, -15 deg C, 30 min, 2.) THF, 4 deg C, 15 h

2: 71 percent / NaOMe / tetrahydrofuran; methanol / 0.5 h / -10 - 20 °C

With 4-methyl-morpholine; sodium methylate; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1016/0223-5234(91)90001-4