C₂₅H₂₈Cl₂F₃N₇O₃S

Base Information

Chemical Name:C₂₅H₂₈Cl₂F₃N₇O₃S
CAS No.:1353628-75-7
Molecular Formula:C₂₅H₂₈Cl₂F₃N₇O₃S
Molecular Weight:634.51
Hs Code.:

C<sub>25</sub>H<sub>28</sub>Cl<sub>2</sub>F<sub>3</sub>N<sub>7</sub>O<sub>3</sub>S

Synonyms:C₂₅H₂₈Cl₂F₃N₇O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₈Cl₂F₃N₇O₃S

Chemical Property:

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Technology Process of C₂₅H₂₈Cl₂F₃N₇O₃S

There total 8 articles about C₂₅H₂₈Cl₂F₃N₇O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353628-61-1
(S)-N-(4-chloro-2-(2-(5,7-dichloropyrazolo[1,5-a]pyrimidin-2-yl)piperidine-1-carbonyl)phenyl)methanesulfonamide

: 13349-90-1
1-(2,2,2-trifluoroethyl)piperazine

: 1353628-75-7
C₂₅H₂₈Cl₂F₃N₇O₃S

Guidance literature:: With sodium carbonate; In water; acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353628-75-7
C₂₅H₂₈Cl₂F₃N₇O₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: sodium methylate / methanol / 5 h / 78 °C

5.1: trichlorophosphate / 3 h / 100 °C

6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

6.2: 0.67 h / 20 °C / Cooling with ice

7.1: sodium carbonate / acetonitrile; water / 3 h / 20 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium carbonate; caesium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; hexanes; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353628-75-7
C₂₅H₂₈Cl₂F₃N₇O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium methylate / methanol / 5 h / 78 °C

4.1: trichlorophosphate / 3 h / 100 °C

5.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

5.2: 0.67 h / 20 °C / Cooling with ice

6.1: sodium carbonate / acetonitrile; water / 3 h / 20 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium carbonate; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;