ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate

Base Information

• Chemical Name: ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate
• CAS No.: 410538-50-0
• Molecular Formula: C₃₀H₂₅N₅O₂
• Molecular Weight: 487.561

Synonyms:ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate

Chemical Property of ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate

Chemical Property:

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Technology Process of ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate

There total 4 articles about ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

ethyl 5-(3-aminophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate (410538-47-5) → ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate (410538-50-0)

Guidance literature:

ethyl 5-(3-aminophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate; With acetic acid; sodium nitrite; In water; at 0 - 5 ℃; for 1h;

With sodium azide; In water; acetic acid; at 20 ℃; for 24h;

DOI:10.1016/S0040-4020(01)01033-X

Reference yield:

3-amino-2,5-diphenylpyrrole (13219-95-9) → ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate (410538-50-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 70 percent / AcOH / Heating

2.1: 70 percent / H₂ / Pd/C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂; acOH / H₂O / 1 h / 0 - 5 °C

3.2: 50 percent / NaN₃ / H₂O; acetic acid / 24 h / 20 °C

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; water;

DOI:10.1016/S0040-4020(01)01033-X

Reference yield:

ethyl 1-(3-nitrophenyl)-1,4-pentanedione-3-carboxylate (118209-48-6) → ethyl 5-(3-azidophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate (410538-50-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 70 percent / AcOH / Heating

2.1: 70 percent / H₂ / Pd/C / ethanol / 20 °C / 2585.74 Torr

3.1: NaNO₂; acOH / H₂O / 1 h / 0 - 5 °C

3.2: 50 percent / NaN₃ / H₂O; acetic acid / 24 h / 20 °C

With hydrogen; acetic acid; sodium nitrite; palladium on activated charcoal; In ethanol; water;

DOI:10.1016/S0040-4020(01)01033-X

upstream raw materials:

ethyl 5-(3-aminophenyl)-1-(2,5-diphenylpyrrol-3-yl)-2-methylpyrrole-3-carboxylate

3-amino-2,5-diphenylpyrrole

ethyl 1-(3-nitrophenyl)-1,4-pentanedione-3-carboxylate

2-methyl-5-(3-nitro-phenyl)-2',5'-diphenyl-1'H-[1,3']bipyrrolyl-3-carboxylic acid ethyl ester

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