4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Base Information

Chemical Name:4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester
CAS No.:1617544-79-2
Molecular Formula:C₃₄H₃₆BNO₂
Molecular Weight:501.476
Hs Code.:

Synonyms:4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Suppliers and Price of 4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

There total 5 articles about 4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1617544-78-1
1-(4-bromophenyl)-1-(4-dimethylaminophenyl)-2,2-diphenylethene

: 1617544-79-2
4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Guidance literature:: 1-(4-bromophenyl)-1-(4-dimethylaminophenyl)-2,2-diphenylethene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c4cc03024a

Reference yield:

: 586-77-6
4-bromo-N,N-dimethylaniline

: 1617544-79-2
4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / 25 °C / Inert atmosphere; Reflux

1.2: 5 h / 0 - 25 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane

3.1: titanium tetrachloride; zinc; pyridine / tetrahydrofuran / -5 - 74 °C / Inert atmosphere

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 - 25 °C / Inert atmosphere

With pyridine; n-butyllithium; titanium tetrachloride; Dess-Martin periodane; magnesium; zinc; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c4cc03024a

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1617544-79-2
4-(1-(4-dimethylaminophenyl)-2,2-diphenylvinyl)phenylboronic acid pinacolester

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / 25 °C / Inert atmosphere; Reflux

1.2: 5 h / 0 - 25 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane

3.1: titanium tetrachloride; zinc; pyridine / tetrahydrofuran / -5 - 74 °C / Inert atmosphere

4.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 4 h / -78 - 25 °C / Inert atmosphere

With pyridine; n-butyllithium; titanium tetrachloride; Dess-Martin periodane; magnesium; zinc; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/c4cc03024a