tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

Base Information

Chemical Name:tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane
CAS No.:192768-03-9
Molecular Formula:C₄₂H₇₀O₁₆Si
Molecular Weight:859.094
Hs Code.:

Synonyms:tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

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Chemical Property of tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

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Technology Process of tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

There total 1 articles about tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 142534-54-1
1D-1-O-(tert-butyldiphenylsilyl)-myo-inositol

: 192768-03-9
tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1016/S0960-894X(97)00197-2

Reference yield: 94.0%

: 192768-03-9
tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

: 192768-04-0
(1R,2S,3S,4R,5R,6S)-2,3,4,5,6-Pentakis-(2-methoxy-ethoxymethoxy)-cyclohexanol

Guidance literature:: With tetraethylammonium fluoride;
DOI:10.1016/S0960-894X(97)00197-2

Reference yield:

: 192768-03-9
tert-Butyl-[(1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-(2-methoxy-ethoxymethoxy)-cyclohexyloxy]-diphenyl-silane

: Octanoic acid (R)-2-[hydroxy-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentahydroxy-cyclohexyloxy)-phosphorylsulfanyl]-1-octanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / tetraethylammonium fluoride

2: tetrazole / tetrahydrofuran / 24 h

3: 65 percent / tetrabutylammonium periodate

4: 1.) Et₃N, 2.) ethanethiol/BF₃ etherate

With 1H-tetrazole; boron trifluoride diethyl etherate; tetraethylammonium fluoride; tetrabutylammonium periodite; triethylamine; ethanethiol; In tetrahydrofuran;
DOI:10.1016/S0960-894X(97)00197-2